Archives / Recipes


Table Of Contents

  1. Methylamine
    1. Synthesis Recipes
      1. Hoffman Rearangement
      2. Schmidt Reaction
      3. Formaldehyde and Ammonia Chloride
      4. Reduction of Nitromethane
      5. Degredation of Hexamine
    2. ZWIT Makes Methylamine Using Hexamine
  2. Isosafrole
    1. Strike's Method
    2. Not-Tim's CaO/KOH
    3. ZWIT Makes Isosafrole Using CaO/KOH
  3. Bromosafrole and Phenylisopropyl Bromide
    1. Strike's Humble Beginnings
    2. Problems and Solutions for HBr
      1. What Is Wrong with 48%aq HBr
      2. Acetic Acid solutions of HBr
      3. 66%aq HBr Solution
      4. Dehydrating 48%aq HBr
        1. Will It Work?
        2. A Proposed Method
      5. Novel Bromination in DSMO
    3. Recipes for Making HBr
      1. KBr / H2SO4 Method
      2. Br2 / SO2 Method
      3. Br2 / S Method
  4. Ya Don't Say
  5. MD-P2Pol & P2Pol
    1. MD-P2Pol & P2Pol part I
      1. Hydrogen Sulfates
      2. Alcohols From Hydrogen Sulfate
      3. Acid Catalyzed Hydration
      4. Acid Catalyzed Dehydration
      5. Dehydration With KHSO4
      6. Other ways to make P2Pols
      7. Conclusion
    2. MD-P2Pol & P2Pol part II
      1. Halogenation of P2Pols
      2. P2Ps from P2Pols
  6. Separation Without Distillation


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